HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → 2-Bromo-6,11-dihydro-N-phenyl-N-methyldibenz[b,e]oxepin-11-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | 2-Bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid | HCID 10403641 | — |
| Product | 2-Bromo-6,11-dihydro-N-phenyl-N-methyldibenz[b,e]oxepin-11-carboxamide | HCID 18998500 | 49.2% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 1.0 g of 2-bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid obtained in Example 46 (Compound H) in place of Compound A and 0.41 g of N-methylaniline in place of aniline to obtain 0.63 g of Compound 43.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478835 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-7fbb97a6458a4aacbd1e2eef0e8a98f1 |
| Source note | uspto-grants-1995_12 |