HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-6-sulfanyl-1,2,3,4-tetrahydroquinolin-2-one → HCID 67623514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-6-sulfanyl-1,2,3,4-tetrahydroquinolin-2-one | HCID 22413759 | — |
| Reactant | HCID 67623996 | HCID 67623996 | — |
| Product | HCID 67623514 | HCID 67623514 | 63% |
Reaction Steps
Using an analogous procedure to that described in Example 6, 6-mercapto-1-methyl-1,2,3,4-tetrahydroquinolin-2-one was reacted with (2SR,4RS)-2-ethyl-4-hydroxy-4-(3-iodophenyl)tetrahydropyran to give (2SR,4RS)-2-ethyl-4-hydroxy-4-[3-(1-methyl-2-oxo-1,2,3,4-tetrahydroquinolin-6-ylthio)phenyl]tetrahydropyran in 63% yield as a gum;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05478842 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-3f5804bbc8394813ae1a731ae225bd4f |
| Source note | uspto-grants-1995_12 |