Phosgene → HCID 10489496, compound

HRID 2260633Notes

Reaction equation

HRID 2260633 reaction equation
[CH2:1]([NH:3][C:4]1[CH:9]=[CH:8][C:7]2[O:10][CH2:11][O:12][C:6]=2[CH:5]=1)[CH3:2].[C:13](Cl)([Cl:15])=[O:14]>>[CH2:1]([N:3]([C:4]1[CH:9]=[CH:8][C:7]2[O:10][CH2:11][O:12][C:6]=2[CH:5]=1)[C:13]([Cl:15])=[O:14])[CH3:2]

Participants

3

Reactant 2

HCID 6371PhosgeneHCID 1183651,3-Benzodioxol-5-amine, N-ethyl-

Product 1

HCID 10489496HCID 10489496, compound

Procedure

By following the procedure described in example 1A, N-ethyl-3,4-methylenedioxyaniline (1.65 g, 10 mmol) was reacted with phosgene to give 1.5 g N-ethyl-N-(3,4-methylenedioxyphenyl)carbamoylchloride. M.p. 68°-69° C.

Sources & evidence

ORD record
ord-b5502747772b4f90a49964f2693cac08
Source dataset
uspto-grants-1995_12
Patent number
US05478845

Reaction notes

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