HCID 54332469, compound → HCID 86749176, compound

HRID 2260718Notes

Reaction equation

HRID 2260718 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:28][CH3:29])=[C:6]([CH:27]=1)[C:7]([NH:9][CH2:10][CH2:11][O:12][C:13]1[CH:26]=[CH:25][C:16]([CH:17]=[C:18]2[S:22][C:21](=[O:23])[NH:20][C:19]2=[O:24])=[CH:15][CH:14]=1)=[O:8]>O1CCOCC1>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:28][CH3:29])=[C:6]([CH:27]=1)[C:7]([NH:9][CH2:10][CH2:11][O:12][C:13]1[CH:26]=[CH:25][C:16]([CH2:17][CH:18]2[S:22][C:21](=[O:23])[NH:20][C:19]2=[O:24])=[CH:15][CH:14]=1)=[O:8]

Participants

3

Reactant 1

HCID 54332469HCID 54332469, compound

Product 1

HCID 86749176HCID 86749176, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

5-(4-[2-(N-(5-Chloro-2-methoxybenzoyl)amino)ethoxy]-benzylidene)-2,4-thiazolidinedione (1.7 g) was dissolved in dioxan (80 ml) and hydrogenated for a total of 22 hours in a manner similar to that described in Example 2. The title compound was obtained as a foam, mp 66-67° C.

Sources & evidence

ORD record
ord-7c3a87002b3d42fdbdfbbf0525711aa6
Source dataset
uspto-grants-1995_12
Patent number
US05478851

Reaction notes

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