反应详情

Under a nitrogen atmosphere, one drop of pyridine was added to 2.0 g of phytanic acid and 10 ml of methylene chloride, and 1.14 g of thionyl chloride was added dropwise at room temperature. After the completion of dropwise addition, the mixture was refluxed for 1 hour, and then concentrated under reduced pressure to obtain about 2 g of phytanic acid chloride.

1. additionwas added dropwise at room temperature
2. additionAfter the completion of dropwise addition
3. temperaturethe mixture was refluxed for 1 hour
4. concentrationconcentrated under reduced pressure