HCID 11676938, compound → HCID 131728555, compound

HRID 2260968Notes

Reaction equation

HRID 2260968 reaction equation
[CH3:1][CH:2]([CH2:17][CH2:18][CH2:19][CH:20]([CH3:32])[CH2:21][CH2:22][CH2:23][CH:24]([CH3:31])[CH2:25][CH2:26][CH2:27][CH:28]([CH3:30])[CH3:29])[CH2:3][CH2:4][CH2:5][C:6]([O:8][CH2:9][C:10]([CH2:15][OH:16])([CH2:13][OH:14])[CH2:11][OH:12])=[O:7]>O>[CH3:1][CH:2]([CH2:17][CH2:18][CH2:19][CH:20]([CH3:32])[CH2:21][CH2:22][CH2:23][CH:24]([CH3:31])[CH2:25][CH2:26][CH2:27][CH:28]([CH3:30])[CH3:29])[CH2:3][CH2:4][CH2:5][C:6]([O:8][CH2:9][C:10]([CH2:13][OH:14])([CH2:11][OH:12])[CH2:15][OH:16])=[O:7].[OH2:7]

Participants

3

Reactant 1

HCID 11676938HCID 11676938, compound

Product 1

HCID 131728555HCID 131728555, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Mono-O-(5,9,13,17-tetramethyloctadecanoyl)pentaerythritol (formula (9) above) and pure water were homogeneously mixed in accordance with the same procedure as in Example 3 to obtain the sample of mono-O-(5,9,13,17-tetramethyloctadecanoyl)pentaerythritol/water system. This sample of mono-O-(5,9,13,17-tetramethyloctadecanoyl)pentaerythritol/water system was subjected to the penetration experiment under a polarizing microscope, SAXS analysis, and dhc value determination based on the results of SAXS analysis in the same manner as in Example 3. As a result, bicontinuous type II Pn3m cubic liquid crystals were found to be stably formed.

Sources & evidence

ORD record
ord-c00394f45d2640518ed4553921ca1d18
Source dataset
uspto-grants-2010_12
Patent number
US07846903B2

Reaction notes

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