HCID 11538038, compound → HCID 131728556, compound
Reaction equation
[CH3:1][CH:2]([CH2:16][CH2:17][CH2:18][CH:19]([CH3:26])[CH2:20][CH2:21][CH2:22][CH:23]([CH3:25])[CH3:24])[CH2:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][C:9]([CH2:14][OH:15])([CH2:12][OH:13])[CH2:10][OH:11]>O>[CH3:1][CH:2]([CH2:16][CH2:17][CH2:18][CH:19]([CH3:26])[CH2:20][CH2:21][CH2:22][CH:23]([CH3:25])[CH3:24])[CH2:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][C:9]([CH2:12][OH:13])([CH2:14][OH:15])[CH2:10][OH:11].[OH2:7]Participants
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Mono-O-(5,9,13-trimethyltetradecyl)pentaerythritol (formula (12) above) and pure water were homogeneously mixed in accordance with the same procedure as in Example 3 to obtain the sample of mono-O-(5,9,13-trimethyltetradecyl)pentaerythritol/water system. The sample of mono-O-(5,9,13-trimethyltetradecyl)pentaerythritol/water system was subjected to the penetration experiment under a polarizing microscope, SAXS analysis, and dhc value determination based on the results of SAXS analysis in the same manner as in Example 3. As a result, bicontinuous type II Pn3m cubic liquid crystals were found to be stably formed at least in a temperature range between 1° C. and 4° C. and at a concentration of 55.3% by mass of mono-O-(5,9,13-trimethyltetradecyl)pentaerythritol.
Sources & evidence
- ORD record
- ord-da6cb29dbeca4a0b8daf435e98e52cfd
- Source dataset
- uspto-grants-2010_12
- Patent number
- US07846903B2
Reaction notes
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