Bromine → HCID 76552553, compound

Participants

Reaction Steps

In a 25 ml 3 neck flask was placed 5-(3-methyl-benzofuran-5-ylmethylene)-thiazolidine-2,4-dione (100 mg, 0.39 mmol) (example 68) and Br2 (20 ul, 1 eq.) in 2 ml of AcOH at 0° C. The mixture was allowed to warm to room temperature. After 2 h at room temperature another equivalent of Br2 was added. After 3 h the reaction was filtered off to obtain a yellow product being the title compound (87 mg, 66%).

Provenance & Evidence