Hexyl isocyanate → HCID 131728558, compound

HRID 2261176Notes

Reaction equation

HRID 2261176 reaction equation
[O:1]1[C:9]2[C:4](=[N:5][CH:6]=[CH:7][CH:8]=2)[NH:3][C:2]1=[O:10].N([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])=C=O>O1CCOCC1>[O:10]=[C:2]1[NH:3][C:4]2=[N:5][CH:6]=[CH:7][CH:8]=[C:9]2[O:1]1.[CH3:19][CH2:18][CH:17]([C:2]([NH2:3])=[O:1])[CH2:16][CH2:15][CH3:14]

Participants

4

Reactant 2

HCID 75659Hexyl isocyanateHCID 2799900Oxazolo(4,5-b)pyridin-2(3H)-one

Product 1

HCID 131728558HCID 131728558, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

100 mg (0.74 mmol) of 3H-oxazolo[4,5-b]pyridin-2-one were reacted in analogy to Example 1 with 102.8 mg (0.809 mmol) of 1-isocyanatohexane in dioxane at 80° C. Yield: 77 mg (40%), M+H+: 264.12.

Sources & evidence

ORD record
ord-25b3dfb443294a1e80e6d45a327fafdf
Source dataset
uspto-grants-2010_12
Patent number
US07846943B2

Reaction notes

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