n-Heptyl isocyanate → HCID 131728559, compound

HRID 2261179Notes

Reaction equation

HRID 2261179 reaction equation
[O:1]1[C:9]2[C:4](=[N:5][CH:6]=[CH:7][CH:8]=2)[NH:3][C:2]1=[O:10].N([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])=C=O>O1CCOCC1>[O:10]=[C:2]1[NH:3][C:4]2=[N:5][CH:6]=[CH:7][CH:8]=[C:9]2[O:1]1.[CH3:20][CH2:19][CH:18]([C:2]([NH2:3])=[O:1])[CH2:17][CH2:16][CH2:15][CH3:14]

Participants

4

Reactant 2

HCID 138341n-Heptyl isocyanateHCID 2799900Oxazolo(4,5-b)pyridin-2(3H)-one

Product 1

HCID 131728559HCID 131728559, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

200 mg (1.47 mmol) of 3H-oxazolo[4,5-b]pyridin-2-one were reacted in analogy to Example 1 with 207 mg (1.47 mmol) of 1-isocyanatoheptane in dioxane at 80° C. Yield: 416 mg (10%), M+H+: 278.15.

Sources & evidence

ORD record
ord-bd92d84937e24327a30be620a9c24d66
Source dataset
uspto-grants-2010_12
Patent number
US07846943B2

Reaction notes

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