HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178510951, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 178509116 | HCID 178509116 | — |
| Reactant | HCID 178509119 | HCID 178509119 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178510951 | HCID 178510951 | — |
Reaction Steps
The title compound (12 mg) was prepared using 130 mg (0.39 mmol) of 4-benzothiazol-2-yl-5-(3-bromopropyl)-2H-pyrazol-3-ylamine, which was derived from 3-(5-amino-4-benzothiazol-2-yl-1H-pyrazol-3-yl)-propan-1-ol, and a saturated solution of ammonia gas in ethanol. MS (m/z, ES+): 274.2 (M+1, 100%), 257.2 (M-NH2, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07847101B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-f54a6427644b4510b3a816393706d268 |
| Source note | uspto-grants-2010_12 |