Ethanolamine → HCID 178434644, compound

HRID 2261700Notes

Reaction equation

HRID 2261700 reaction equation
Br[CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[N:7]=[C:8]([C:10]3[C:14]([CH3:15])=[N:13][NH:12][C:11]=3[NH2:16])[S:9][C:5]=2[CH:4]=1.[NH2:19][CH2:20][CH2:21][OH:22]>>[NH2:16][C:11]1[NH:12][N:13]=[C:14]([CH3:15])[C:10]=1[C:8]1[S:9][C:5]2[CH:4]=[C:3]([CH2:2][NH:19][CH2:20][CH2:21][OH:22])[CH:18]=[CH:17][C:6]=2[N:7]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 178434639HCID 178434639, compound

Product 1

HCID 178434644HCID 178434644, compound

Procedure

The title compound (10 mg) was prepared starting from 40 mg of 4-(6-bromomethylbenzothiazol-2-yl)-5-methyl-2H-pyrazol-3-ylamine and excess 2-aminoethanol. MS (m/z, ES+): 304.1 (M+1, 10%), 243.2 (M-HOCH2CH2NH, 100%).

Sources & evidence

ORD record
ord-84036ce4284a44e2b92f8db8d3d6afb6
Source dataset
uspto-grants-2010_12
Patent number
US07847101B2

Reaction notes

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