2-(Trifluoromethoxy)aniline → HCID 53415749, compound

HRID 2261736Notes

Reaction equation

HRID 2261736 reaction equation
[ClH:1].FC(F)(F)O[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[NH:11][NH2:12].[F:15][C:16]([F:26])([F:25])[O:17]C1C=CC=CC=1N>>[ClH:1].[F:15][C:16]([F:26])([F:25])[O:17][N:11]([C:6]1[CH:5]=[CH:10][CH:9]=[CH:8][CH:7]=1)[NH2:12]

Participants

3

Reactant 2

HCID 737542-(Trifluoromethoxy)anilineHCID 19889891[2-(Trifluoromethoxy)phenyl]hydrazine--hydrogen chloride (1/1)

Product 1

HCID 53415749HCID 53415749, compoundYield 54%

Procedure

The title compound (115.8 g, 54%) is prepared essentially according to the preparation of (2-trifluoromethoxy-phenyl)-hydrazine hydrochloride using 2-trifluoromethoxy-phenylamine.

Sources & evidence

ORD record
ord-4a0271f86d4d402f9d7d196efab20d1b
Source dataset
uspto-grants-2010_12
Patent number
US07846960B2

Reaction notes

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