HRID2261755

反应详情

EQUATION

反应方程式

HRID 2261755 的结构方程式

PROCEDURE

实验过程

The title compound (292 mg, quantitative yield) is prepared essentially according to the preparation of 2-{4-[2-(2,6-Dichloro-phenyl)-4-isopropyl-2H-pyrazol-3-ylmethoxy]-2-methyl-phenyl}-propionaldehyde using 1-(2,6-dichloro-phenyl)-4-isopropyl-5-[4-(2-methoxy-vinyl)-3-methyl-phenoxymethyl]-1H-pyrazole. 1H NMR (400 MHz, CDCl3) δ 9.65 (t, 1H, J=2.2 Hz), 7.70 (s, 1H), 7.41 (d, 2H, J=8.4 Hz), 7.31 (dd, 1H, J=8.8, 7.4 Hz), 6.98 (d, 1H, J=7.9 Hz), 6.65-6.58 (m, 2H), 4.80 (s, 2H), 3.60 (d, 2H, J=2.2 Hz), 3.00 (sept, 1H, J=7.0 Hz), 2.18 (s, 3H), 1.31 (d, 6H, J=7.0 Hz).