Sulfuric Acid → Titanium disulfate
Reaction equation
[Ti:1].[S:2](=[O:6])(=[O:5])([OH:4])[OH:3]>>[S:2]([O-:6])([O-:5])(=[O:4])=[O:3].[Ti+4:1].[S:2]([O-:6])([O-:5])(=[O:4])=[O:3]Participants
Reactant 2
Product 1
Procedure
A titanium-containing ore was dissolved with sulfuric acid to obtain a titanium sulfate solution. The titanium sulfate solution was hydrolyzed to obtain hydrous titanium oxide. Subsequently, 0.50 parts by mass of ammonium phosphate, 0.30 parts by mass of potassium sulfate, and 0.30 parts by mass of aluminum sulfate were added to 100 parts by mass of the hydrous titanium oxide in terms of TiO2. The hydrous titanium oxide was heated in a laboratory rotary muffle furnace until the temperature of the resulting product reached 1,020° C. Titanium dioxide fine particles produced were cooled to room temperature, and observed with a transmission electron micrograph. According to the result, it was found that the fine particles were anatase TiO2 particles having an average primary particle diameter of 0.13 μm.
Sources & evidence
- ORD record
- ord-082ac1f2db314cfc9ba62176ec87c12d
- Source dataset
- uspto-grants-2010_12
- Patent number
- US07850773B2
Reaction notes
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