Diisopropylcarbodiimide → HCID 68781363, compound

Participants

Reaction Steps

18.0 g of N-lauroyl-L-glutamine was dissolved in 52.6 mL of dimethylformamide, and 5.50 g of 1-hydroxybenzotriazole was added to it, then 6.90 g of diisopropylcarbodiimide was added thereto and reacted at 50° C. Dimethylformamide was concentrated under reduced pressure, then the reaction mixture was suspended in methanol, the insoluble matter was collected by filtration to obtain 7.88 g of 2-(lauroylamino)glutarimide.

Provenance & Evidence