HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → HCID 25131771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | HCID 178505600 | HCID 178505600 | — |
| Product | HCID 25131771 | HCID 25131771 | 71% |
Reaction Steps
As described for Example 24, 3-(4-fluoro-phenyl)-4-(1H-imidazol-4-yl)-5-trifluoromethyl-isoxazole (100 mg, 0.34 mmol), using 1-fluoro-4-nitrobenzene instead of 4-fluoroacetophenone, was converted to the title compound (100 mg, 71%) which was obtained as a yellow solid. MS: m/e=417.1 [M−H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851469B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-ce94dea9c3a44fdea3c38663a11d2a92 |
| Source note | uspto-grants-2010_12 |