HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Chloropyridin-3-yl)ethan-1-one → HCID 25132819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Chloropyridin-3-yl)ethan-1-one | HCID 2779698 | — |
| Reactant | HCID 178505600 | HCID 178505600 | — |
| Product | HCID 25132819 | HCID 25132819 | 38% |
Reaction Steps
As described for Example 24, 3-(4-fluoro-phenyl)-4-(1H-imidazol-4-yl)-5-trifluoromethyl-isoxazole (120 mg, 0.4 mmol), using 1-(6-chloro-3-pyridinyl)-1-ethanone instead of 4-fluoroacetophenone, was converted to the title compound (64 mg, 38%) which was obtained as a light yellow solid. MS: m/e=417.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851469B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-98516bb1387f4ecd911d869ca94b8a64 |
| Source note | uspto-grants-2010_12 |