反应详情

A mixture of 5.5 g (36 mmol) of methyl 3-methylbenzoate, 7.1 g (39.5 mmol) of N-Bromosuccinimide and 0.44 g (1.8 mmol) of benzoyl peroxide in 75 ml of Cl4C is refluxed for 5 h. The solid is filtered and washed with Cl4C. The mother liquors are concentrated and a yellow solid is obtained which is, essentially, monobromated product. This is used in the next step without further purification.

1. temperatureis refluxed for 5 h
2. filtrationThe solid is filtered
3. washwashed with Cl4C
4. concentrationThe mother liquors are concentrated
5. customa yellow solid is obtained which
6. customThis is used in the next step without further purification