Water → HCID 86245184, compound

Participants

Reaction Steps

To a solution of 2-aminobenzothiazole (1.00 g, 6.66 mmol) and pyridine (0.633 ml, 7.99 mmol) in tetrahydrofuran (22 ml) was added, under ice-cooling, 2,2,2-trichloroethyl chloroformate (1.11 ml, 7.99 mmol), and the mixture was stirred at room temperature for 1 hour. Water was poured to the reaction mixture, and 1.19 g (54.7%) of the desired product as a solid was separated by filtration.

Provenance & Evidence