HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 57438791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 17895683 | HCID 17895683 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 57438791 | HCID 57438791 | — |
Reaction Steps
A mixture of 4-(2,3-dichlorophenyl)piperidine (20 mg, 0.064 mmol), 1,2-dichloroethane (1 ml), glacial acetic acid (4 mg, 0.064 mmol), paraformaldehyde (2 mg, 0.066 mmol) and sodium triacetoxyborohydride (20 mg, 0.092 mmol) was stirred 15 h at ambient temperature. MS m/z (rel. intensity, 70 eV) 244 (M+, 68), 243 (54), 242 (bp), 208 (61), 115 (29).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851629B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-13d3e2b62bf14247991b41921be1bea4 |
| Source note | uspto-grants-2010_12 |