HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylaluminum → HCID 178466274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Reactant | Methyl 4-tert-butyl-2-ethoxybenzoate | HCID 53412323 | — |
| Reactant | HCID 58006923 | HCID 58006923 | — |
| Product | HCID 178466274 | HCID 178466274 | — |
Reaction Steps
In a manner analogous to the method described in example 2, rac-(1R*,2S*)-1,2-bis-(4-chloro-phenyl)-propane-1,2-diamine was reacted with 4-tert-butyl-2-ethoxy-benzoic acid methyl ester (prepared as described in Fotouhi, N. et al. WO 2005110996) in the presence of trimethylaluminum to give the title compound as a racemic mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07851626B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-1c9d32eedc8040329246eeda4b62d89f |
| Source note | uspto-grants-2010_12 |