HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59596015, compound → HCID 59595986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59596015 | HCID 59596015 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59595986 | HCID 59595986 | 98.1% |
Reaction Steps
A suspension of 5-nitro-2-(1,3-oxazol-2-yl)-3,4′-bipyridin-6-amine (0.089 g, 0.31 mmol) and palladium on carbon (10%, 20 mg) in ethanol (15 mL) was placed under a hydrogen atmosphere (balloon) and stirred at room temperature. After 3 hours, the mixture was filtered through Celite® and the filtrate was evaporated. Trituration with diethyl ether gave the title compound (0.077 g, 97%) as a pale orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855202B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-e57fe1f34ca0402585c6297631c2564a |
| Source note | uspto-grants-2010_12 |