3,4,5-Trimethoxyaniline → HCID 24860829, compound

Participants

Reaction Steps

Using the procedure of example 1, 3,4,5-trimethoxyaniline (158 mg) was reacted with compound 1f (100 mg) to provide compound 2 (35 mg, 34%). 1H NMR (400 MHz, CD3OD) δ 8.82 (d, J=8.0 Hz, 1H), 8.33 (d, J=5.2 Hz, 1H), 8.31 (d, J=4.8 Hz, 1H), 8.11 (s, 1H), 7.48 (s, 2H), 7.22 (dd, J=8.0 Hz, 4.8 Hz, 1H), 7.12 (d, J=4.8 Hz, 1H), 3.86 (s, 9H). MS (ESI) m/z: 378 (M+H)+.

Provenance & Evidence