P-Anisidine → HCID 58692220, compound

Participants

Reaction Steps

Using the procedure of example 1, p-anisidine (100 mg) was reacted with compound 1f (100 mg) to provide compound 5 (35 mg, 41%). 1H NMR (400 MHz, CD3OD) δ 8.73 (d, J=8.0 Hz, 1H), 8.27 (m, 2H), 8.07 (s, 1H), 7.55 (d, J=9.0 Hz, 2H), 7.18 (dd, J=8.0 Hz, 4.8 Hz, 1H), 7.06 (d, J=5.6 Hz, 1H), 6.96 (d, J=9.0 Hz, 2H), 3.86 (s, 3H). MS (ESI) m/z: 318 (M+H)+.

Provenance & Evidence