3-Methoxyaniline → HCID 15952398, compound

Participants

Reaction Steps

Using the procedure of example 1, m-anisidine (100 mg) was reacted with compound 1f (100 mg) to provide compound 6 (25 mg, 29%). 1H NMR (400 MHz, CD3OD) δ 8.84 (d, J=8.0 Hz, 1H), 8.33 (d, J=5.2 Hz, 1H), 8.31 (d, J=4.8 Hz, 1H), 8.12 (s, 1H), 7.48 (m, 1H), 7.30 (t, J=8.0 Hz, 1H), 7.23 (m, 2H), 7.13 (d, J=5.2 Hz, 1H), 6.68 (d, J=8.0 Hz, 1H), 3.86 (s, 3H). MS (ESI) m/z: 318 (M+H)+.

Provenance & Evidence