2-Methoxyaniline → HCID 44416017, compound

Participants

Reaction Steps

Using the procedure of example 1, o-anisidine (100 mg) was reacted with compound 1f (100 mg) to provide compound 7 (20 mg, 24%). 1H NMR (400 MHz, CD3OD) δ 8.81 (d, J=8.0 Hz, 1H), 8.40 (m, 1H), 8.33 (d, J=4.8 Hz, 1H), 8.30 (d, J=4.8 Hz, 1H), 8.20 (s, 1H), 7.23 (dd, J=8.0 Hz, 4.8 Hz, 1H), 7.20 (d, J=5.2 Hz, 1H), 7.08-7.01 (m, 3H), 3.97 (s, 3H). MS (ESI) m/z: 318 (M+H)+.

Provenance & Evidence