O-Toluidine → HCID 44416088, compound

Participants

Reaction Steps

Using the procedure of example 1, o-toluidine (87 mg) was reacted with compound 1f (100 mg) to provide compound 8 (27 mg, 33%). 1H NMR (400 MHz, CD3OD) δ 8.55 (d, J=8.0 Hz, 1H), 8.24 (d, J=5.2 Hz, 1H), 8.12 (s, 1H), 7.69 (d, J=7.6 Hz, 1H), 7.29 (q, J=7.6 Hz, 1H), 7.18 (d, J=7.2 Hz, 1H), 7.11 (d, J=5.6 Hz, 1H), 7.11 (dd, J=7.6 Hz, 4.8 Hz, 1H), 2.35 (s, 3H). MS (ESI) m/z: 302 (M+H)+.

Provenance & Evidence