p-Toluidine → HCID 44415976, compound

Participants

Reaction Steps

Using the procedure of example 1, p-toluidine (87 mg) was reacted with compound 1f (100 mg) to provide compound 10 (35 mg, 43%). 1H NMR (400 MHz, CD3OD) δ 8.82 (d, J=8.0 Hz, 1H), 8.28 (m, 2H), 8.13 (s, 1H), 7.62 (s, 1H), 7.56 (d, J=8.0 Hz, 2H), 7.21 (m, 2H), 7.12 (d, J=5.2 Hz, 1H), 2.38 (s, 3H). MS (ESI) m/z: 302 (M+H)+.

Provenance & Evidence