2-Chloroaniline → HCID 44416064, compound

Participants

Reaction Steps

Using the procedure of example 1, 2-chloro-aniline (103 mg) was reacted with compound 1f (100 mg) to provide compound 12 (17 mg, 20%). 1H NMR (400 MHz, CD3OD) δ 8.75 (d, J=7.6 Hz, 1H), 8.39 (d, J=8.4 Hz, 1H), 8.36 (d, J=5.2 Hz, 1H), 8.30 (d, J=4.8 Hz, 1H), 8.20 (s, 1H), 7.49 (d, J=7.6 Hz, 1H), 7.38 (t, J=8.0 Hz, 1H), 7.25 (d, J=5.2 Hz, 1H), 7.22 (dd, J=7.6 Hz, 4.8 Hz, 1H), 7.12 (t, J=7.6 Hz, 1H). MS (ESI) m/z 322: (M+H)+.

Provenance & Evidence