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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2264245Generated: October 31, 2026

Cyclohexylamine → HCID 44415977, compound

https://huagongshe.com/reaction/2264245

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexylamineHCID 7965—
ReactantHCID 59596028HCID 59596028—
ProductHCID 44415977HCID 4441597742%

Reaction Steps

Using the procedure of example 1, cyclohexylamine (88 mg) was reacted with compound 1f (100 mg) to provide compound 13 (33 mg, 42%). 1H NMR (400 MHz, CD3OD) δ 8.91 (d, J=8.4 Hz, 1H), 8.26 (d, J=4.8 Hz, 1H), 8.16 (s, 1H), 8.10 (d, J=5.6 Hz, 1H), 7.22 (dd, J=8.0 Hz, 4.8 Hz, 1H), 6.97 (d, J=5.6 Hz, 1H), 3.86 (m, 1H), 2.13-1.27 (m, 10H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07855205B2
Source datasetuspto-grants-2010_12
ORD IDord-33becbd4519c47e6967ba20c6cef99e7
Source noteuspto-grants-2010_12