HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 44415977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 59596028 | HCID 59596028 | — |
| Product | HCID 44415977 | HCID 44415977 | 42% |
Reaction Steps
Using the procedure of example 1, cyclohexylamine (88 mg) was reacted with compound 1f (100 mg) to provide compound 13 (33 mg, 42%). 1H NMR (400 MHz, CD3OD) δ 8.91 (d, J=8.4 Hz, 1H), 8.26 (d, J=4.8 Hz, 1H), 8.16 (s, 1H), 8.10 (d, J=5.6 Hz, 1H), 7.22 (dd, J=8.0 Hz, 4.8 Hz, 1H), 6.97 (d, J=5.6 Hz, 1H), 3.86 (m, 1H), 2.13-1.27 (m, 10H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855205B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-33becbd4519c47e6967ba20c6cef99e7 |
| Source note | uspto-grants-2010_12 |