2-Bromoaniline → HCID 44416087, compound

Participants

Reaction Steps

Using the procedure of example 1, 2-bromoaniline (139 mg) was reacted with compound 1f (100 mg) to provide compound 28 (23 mg, 23%). 1H NMR (400 MHz, CD3OD) δ 8.67 (d, J=8.0 Hz, 1H), 8.30 (t, J=5.2 Hz, 1H), 8.25 (d, J=1.2 Hz, 1H), 8.24 (s, 1H), 8.15 (d, J=8.0 Hz, 1H), 7.67 (d, J=8.0 Hz, 1H), 7.41 (t, J=8.0 Hz, 1H), 7.26 (d, J=6.0 HZ, 1H), 7.15 (dd, J=7.8 Hz, 4.8 Hz, 1H), 7.08 (t, J=7.8 Hz, 1H). MS (ESI) m/z: 366 (M+H)+.

Provenance & Evidence