2-Fluoroaniline → HCID 44416036, compound

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Reaction Steps

Using the procedure of example 1, 2-fluoroaniline (90 mg) was reacted with compound 1f (100 mg) to provide compound 31 (45 mg, 55%). 1H NMR (400 MHz, CD3OD) δ 8.73 (d, J=8.0 Hz, 1H), 8.29 (d, J=5.2 Hz, 1H), 8.26 (m, 1H), 8.24 (s, 1H), 8.04 (t, J=8.0 Hz, 1H), 7.25 (d, J=5.6 Hz, 1H), 7.22-7.14 (m, 4H). MS (ESI) m/z: 306 (M+H)+.

Provenance & Evidence