2,4-Dimethylaniline → HCID 58692224, compound

Participants

Reaction Steps

Using the procedure of example 1, 2,4-dimethylaniline (98 mg) was reacted with compound 1f (100 mg) to provide compound 33 (37 mg, 44%). 1H NMR (400 MHz, CD3OD) δ 8.50 (d, J=8.0 Hz, 1H), 8.21 (d, J=4.8 Hz, 1H), 8.18 (s, 1H), 8.17 (d, J=5.6 Hz, 1H), 7.36 (d, J=8.0 Hz, 1H), 7.14 (s, 1H), 7.12 (d, J=5.6 Hz, 1H), 7.07 (d, J=8.0 Hz, 1H), 7.03 (dd, J=8.0 Hz, 4.8 Hz, 1H), 2.38 (s, 3H), 2.26 (s, 3H). MS (ESI) m/z: 316 (M+H)+.

Provenance & Evidence