2,3-Dimethylaniline → HCID 58692249, compound

Participants

Reaction Steps

Using the procedure of example 1, 2,3-dimethylaniline (98 mg) was reacted with compound 1f (100 mg) to provide compound 34 (50 mg, 59%). 1H NMR (400 MHz, CD3OD) δ 8.42 (d, J=8.0 Hz, 1H), 8.21 (d, J=4.8 Hz, 1H), 8.19 (s, 1H), 8.17 (d, J=5.2 Hz, 1H), 7.27 (d, J=7.2 Hz, 1H), 7.18-7.13 (m, 3H), 7.02 (dd, J=8.0 Hz, 4.8 Hz, 1H), 2.37 (s, 3H), 2.20 (s, 3H). MS (ESI) m/z: 316 (M+H)+.

Provenance & Evidence