2,6-Dimethylaniline → HCID 58692207, compound

Participants

Reaction Steps

Using the procedure of example 1, 2,6-dimethylaniline (98 mg) was reacted with compound 1f (100 mg) to provide compound 35 (34 mg, 40%). 1H NMR (400 MHz, CD3OD) δ 8.40 (d, J=8.0 Hz, 1H), 8.21 (d, J=4.8 Hz, 1H), 8.19 (s, 1H), 8.17 (d, J=5.2 Hz, 1H), 7.50 (d, J=7.2 Hz, 1H), 7.35 (d, J=7.2 Hz, 1H), 7.14 (d, J=5.2 Hz, 2H), 7.03 (t, J=5.2 Hz, 1H), 2.36 (s, 6H). MS (ESI) m/z: 316 (M+H)+.

Provenance & Evidence