2,4-Dichloroaniline → HCID 56659827, compound

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Reaction Steps

Using the procedure of example 1, 2,4-dichloroaniline (131 mg) was reacted with compound 1f (100 mg) to provide compound 36 (47 mg, 49%). 1H NMR (400 MHz, CD3OD) δ 8.69 (d, J=8.0 Hz, 1H), 8.33 (d, J=4.8 Hz, 1H), 8.26 (d, J=5.6 Hz, 1H), 8.23 (s, 1H), 8.20 (d, J=8.0 Hz, 1H), 7.57 (s, 1H), 7.36 (d, J=5.6 Hz, 1H), 7.30 (d, J=8.0 Hz, 1H), 7.18 (dd, J=8.0 Hz, 4.8 Hz, 1H). MS (ESI) m/z: 356 (M+H)+.

Provenance & Evidence