N,N-dimethyl-p-phenylenediamine → HCID 58692251, compound

Participants

Reaction Steps

Using the procedure of example 1, N,N-dimethyl-p-phenylenediamine (221 mg) was reacted with compound 1f (100 mg) to provide compound 38 (52 mg, 29%). 1H NMR (400 MHz, CD3OD) δ 8.85 (d, J=8.0 Hz, 1H), 8.25 (d, J=8.0 Hz, 1H), 8.20 (s, 1H), 8.18 (d, J=4.8 Hz, 1H), 7.45 (d, J=8.0 Hz, 1H), 7.43 (m, 1H), 7.18 (dd, J=8;0 Hz, 5.6 Hz, 1H), 7.12 (d, J=5.6 Hz, 1H), 6.88 (d, J=8.0 Hz, 1H), 6.85 (d, J=8.0 Hz, 1H), 2.90 (s, 6H).

Provenance & Evidence