4-Aminophenol → HCID 58692226, compound

Participants

Reaction Steps

Using the procedure of example 1, 4-aminophenol (177 mg) was reacted with compound 1f (200 mg) to provide compound 39 (48 mg, 29%). 1H NMR (400 MHz, CD3OD) δ 8.48 (d, J=8.0 Hz, 1H), 8.24 (s, 1H), 8.23 (d, J=8.0 Hz, 1H), 8.12 (d, J=4.8 Hz, 1H), 7.45 (d, J=8.0 Hz, 1H), 7.05 (dd, J=8.0 Hz, 5.6 Hz, 1H), 7.00 (d, J=5.2 Hz, 1H), 6.98 (m, 1H), 6.85 (d, J=8.0 Hz, 1H), 6.83 (d, J=8.0 Hz, 1H). MS (ESI) m/z: 304 (M+H)+.

Provenance & Evidence