4-Ethoxyaniline → HCID 58692221, compound

Participants

Reaction Steps

Using the procedure of example 1, 4-ethoxyaniline (222 mg) was reacted with compound 1f (200 mg) to provide compound 40 (55 mg, 31%). 1H NMR (400 MHz, DMSO) δ 8.90 (d, J=8.0 Hz, 1H), 8.45 (s, 1H), 8.30 (d, J=5.6 Hz, 2H), 7.66 (d, J=8.0 Hz, 2H), 7.25 (d, J=5.6 Hz, 1H), 7.20 (m, 1H), 6.90 (d, J=8.0 Hz, 2H), 4.05 (q, J=8.0 Hz, 2H), 1.36 (t, J=8.0 Hz, 3H). MS (ESI) m/z: 332 (M+H)+.

Provenance & Evidence