4-Amino-m-cresol → HCID 58692217, compound

Participants

Reaction Steps

Using procedure of example 1, compound 1f (4.0 g) was reacted with 4-amino-3-methylphenol (2.66 g) to provide 1.7 g (50%) of compound 79. 1H NMR (400 MHz, DMSO) δ 12.20 (s, 1 H), 9.18 (s, 1 H), 8.45 (s, 1 H), 8.35 (d, 1 H), 8.22 (d, 1 H), 8.18 (d, 1 H), 7.15 (m, 1 H), 7.00 (m, 1 H), 6.65 (d, 1 H), 6.60 (dd, 1 H), 2.15 (s, 3 H). MS (ESI) m/z: 316 (M+H)+.

Provenance & Evidence