HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 23112247, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide | HCID 15908 | — |
| Reactant | 4-((Tert-butoxy)carbonyl)morpholine-2-carboxylic acid | HCID 2755965 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23112247 | HCID 23112247 | — |
Reaction Steps
4-(t-Butoxycarbonyl)morpholine-2-carboxylic acid and diethylamine were dissolved in DMF, 1-ethyl-3-(3′-dimethylaminopropyl)carbodiimide was added thereto at room temperature, and the whole was stirred to obtain t-butyl 2-[(diethylamino)carbonyl]morpholine-4-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07855198B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-408ce7c447634cf0b8140e609783c84a |
| Source note | uspto-grants-2010_12 |