Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzamide | HCID 2331 | — |
| Reactant | 5-Isocyanato-1,2,3-trimethoxybenzene | HCID 517766 | — |
| Product | HCID 68783913 | HCID 68783913 | 76% |
Reaction Steps
A mixture of benzamide (0.5 g, 4.13 mmol, 1.0 equiv) and 5-isocyanato-1,2,3-trimethoxy-benzene (1.30 g, 6.19 mmol, 1.5 equiv; commercially available) was heated by microwave irradiation to 140° C. for 30 min. Recrystallization from ethanol provided 1.04 g (76%) of the title compound. MS (ISP): 331.3 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07855194B2 |
|---|
| Source dataset | uspto-grants-2010_12 |
|---|
| ORD ID | ord-20750f28c23b4783b7cbeac4fc7f1a28 |
|---|
| Source note | uspto-grants-2010_12 |
|---|
