Hydrochloric Acid → HCID 68779308, compound

Participants

Reaction Steps

A solution of 4-(4,6-dimethoxy-[1,3,5]triazin-2-ylamino)-piperidine-1-carboxylic acid tert-butyl ester (2.60 g, 7.66 mmol) in 4 M HCl in dioxane (100 mL) was stirred at 0° C. for 1 h. The solvent was removed under reduced pressure and the crude product used in the consecutive step without further purification assuming quantitative deprotection and formation of the dihydrochloride salt. MS (ISP): 240.4 [M+H]+.

Provenance & Evidence