2-Methylbenzothiazole → HCID 178476295, compound

HRID 2264859Notes

Reaction equation

HRID 2264859 reaction equation
[CH3:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[I:11][CH2:12][CH2:13][CH2:14][CH2:15][O:16][C:17](=[O:19])[CH3:18]>CCOCC>[I-:11].[C:17]([O:16][CH2:15][CH2:14][CH2:13][CH2:12][SH:3]1[C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[NH+:6]=[C:2]1[CH3:1])(=[O:19])[CH3:18]

Participants

4

Reactant 2

HCID 84462-MethylbenzothiazoleHCID 27334054-Iodobutyl acetate

Product 1

HCID 178476295HCID 178476295, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

10 mmol (1.49 g) 2-methyl-benzothiazole and 10 mmol (2.42 g) 4-iodobutylacetate are heated for 4 h at 120° C. and after cooling mixed with ether sucked off, again washed with ether and dried in vacuum.

Workup

  1. temperatureafter cooling
  2. washagain washed with ether
  3. customdried in vacuum

Sources & evidence

ORD record
ord-a477ee4c7aa143adac748e8534509a7d
Source dataset
uspto-grants-2010_12
Patent number
US07855293B2

Reaction notes

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