HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(E)-Ethyl 3-(4-aminophenyl)-2-methylacrylate → (E)-Ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]phenyl]-2-methylacrylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (E)-Ethyl 3-(4-aminophenyl)-2-methylacrylate | HCID 15086587 | — |
| Edukt | Ethyl 4-[[3,5-bis(trimethylsilyl)benzoyl]amino]-2-fluorocinnamate | HCID 68484203 | — |
| Produkt | (E)-Ethyl 3-[4-[[3,5-bis(trimethylsilyl)benzoyl]amino]phenyl]-2-methylacrylate | HCID 86644283 | 27% |
Reaktionsschritte
Using BTMB (1.95 g) and Compound 13a (1.8 g), Compound 13b (910 mg, 27%) was obtained as a yellow solid in the same manner as Compound 2b was synthesized.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07855300B2 |
| Quelldatensatz | uspto-grants-2010_12 |
| ORD ID | ord-4f793bf68ab140ebbf559f9fc441df93 |
| Quellennotiz | uspto-grants-2010_12 |