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HRID2265189

反应详情

EQUATION

反应方程式

HRID 2265189 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1cccc2nsnc12
HCID2735459

2,1,3-Benzothiadiazole, 4-chlorosulfonyl-

C6H3ClN2O2S2

结构：COC(=O)c1ccc(C)cc1N
HCID11205965

Methyl 2-amino-4-methylbenzoate

C9H11NO2

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(C)cc1NS(=O)(=O)c1cccc2nsnc12
HCID68770725

未命名化合物

收率 53%

PROCEDURE

实验过程

The title compound (1.22 g, 53%) was prepared from benzo[1,2,5]thiadiazole-4-sulfonyl chloride and 2-amino-4-methyl-benzoic acid methyl ester as in Example 10, Part A. 1H NMR (500 MHz, CDCl3): 11.28 (s, 1H), 8.36 (dd, J=7.1, 1.0, 1H), 8.19 (dd, J=8.8, 1.0, 1H), 7.73 (d, J=8.1, 1H), 7.68 (dd, J=8.8, 7.1, 1H), 7.51 (br s, 1H), 6.77 (dd, J=8.1, 0.9, 1H), 3.89 (s, 3H), 2.28 (s, 3H).