Diethylethanolamine → HCID 68680152, compound

HRID 2265886Notes

Reaction equation

[OH:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]([C:12]([O:14][CH3:15])=[O:13])[N:7]([S:16]([C:19]1[CH:24]=[CH:23][C:22]([O:25][C:26]3[CH:31]=[CH:30][C:29]([O:32][CH3:33])=[CH:28][CH:27]=3)=[CH:21][CH:20]=1)(=[O:18])=[O:17])[CH2:6][CH2:5]2.[CH2:34]([N:36]([CH2:40][CH3:41])[CH2:37][CH2:38]O)[CH3:35].FC1C=CC(OC2C=CC(S(N3CCC4C(=CC=C(OCCCN5CCN(C)CC5)C=4)C3C(OC)=O)(=O)=O)=CC=2)=CC=1>>[CH2:34]([N:36]([CH2:40][CH3:41])[CH2:37][CH2:38][O:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]([C:12]([O:14][CH3:15])=[O:13])[N:7]([S:16]([C:19]1[CH:24]=[CH:23][C:22]([O:25][C:26]3[CH:27]=[CH:28][C:29]([O:32][CH3:33])=[CH:30][CH:31]=3)=[CH:21][CH:20]=1)(=[O:17])=[O:18])[CH2:6][CH2:5]2)[CH3:35]

Participants

Reactant 3

HCID 7497Diethylethanolamine

HCID 68679430HCID 68679430, compound

HCID 68680121HCID 68680121, compound

Product 1

HCID 68680152HCID 68680152, compound

Procedure

Methyl 6-hydroxy-2-[4-(4-methoxyphenoxy)benzenesulfonyl]-1,2,3,4-tetrahydroiso-quinoline-1-carboxylate (13B) is reacted with 2-diethylaminoethanol by the method described under 3C.

Sources & evidence

ORD record: ord-eabcbaaa80884860b8df5d28ba835aa2
Source dataset: uspto-grants-2010_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07858619B2

Reaction notes

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