Triphenylphosphine → HCID 66879410, compound

Participants

Reaction Steps

200 mg (0.516 mmol) of 4-(4-fluorophenoxy)-N-[2-(2-hydroxyphenyl)ethyl]benzene-sulfonamide are reacted in 20 ml of THF with 230 mg (0.878 mmol) of triphenyl-phosphine, 141 μl (0.774 mmol) of DEAD and 0.165 ml (1.239 mmol) of 2-piperidin-1-ylethanol in analogy to the method described under 3C, resulting in the title compound in a yield of 69%.

Provenance & Evidence