HCID 6465104, compound → HCID 68680371, compound
Reaction equation
C[O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:9][CH2:10][NH:11][S:12]([C:15]1[CH:20]=[CH:19][C:18]([CH3:21])=[CH:17][CH:16]=1)(=[O:14])=[O:13].FC1C=CC(OC2C=CC(S(NCCC3C=CC=CC=3O)(=O)=O)=CC=2)=CC=1>>[OH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:9][CH2:10][NH:11][S:12]([C:15]1[CH:16]=[CH:17][C:18]([CH3:21])=[CH:19][CH:20]=1)(=[O:14])=[O:13]Participants
3
Procedure
The title compound is prepared starting from N-[2-(2-methoxyphenyl)ethyl]-4-methylbenzenesulfonamide in analogy to the method described under 19B, it likewise being possible for the crude product to be reacted further without further purification.
Workup
- customto be reacted further without further purification
Sources & evidence
- ORD record
- ord-6def471736164d988dd9ede3fd8e3eb6
- Source dataset
- uspto-grants-2010_12
- Patent number
- US07858619B2
Reaction notes
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